Analytical and Organic Chemistry" is designed for B.Sc. students of Chemistry (First Semester) of Karnataka State Higher Education Council (KSHEC) as per the recommended National Education Policy (NEP) 2020. It covers important topics such as Language of Analytical Chemistry, Titrimetric Analysis, Classification and Nomenclature of Organic Compounds, Nature of Bonding in Organic Molecules, Mechanisms of Organic Reactions, Chemistry of Alkanes, Alkenes, Nucleophilic Substitution and Aromaticity and Aromatic Hydrocarbons. Laboratory Work includes experiments on both Analytical and Organic Chemistry and contains Calibration of Glassware, Acid-Alkali, Potassium Dichromate, Potassium Permanganate and EDTA Titrations along with Selection of suitable solvents for Purification/Crystallization of Organic Compounds as well as Organic Preparations.